The synergistic effect of phosphomolybdic acid on rhodium-based metal-organic frameworks for the efficient selective photocatalytic reduction of CO2to CO

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成果类型：

期刊论文

作者：

Shan, Yurong;Liu, Dexiang;Xu, Chunyan;Zhan, Peng;Wang, Hui;...

通讯作者：

Wang, Hui(wh9469@126.com)

作者机构：

[Zhan, Peng; Xu, Chunyan; Shan, Yurong; Wang, Hui; Liu, Dexiang] Cent South Univ Forestry & Technol, Sch Mat Sci & Engn, Changsha 410004, Peoples R China.

[Wang, Wenlei; Wang, Jing; He, Ren] Cent South Univ Forestry & Technol, Coll Sci, Changsha 410004, Peoples R China.

通讯机构：

[Hui Wang] S

[Wenlei Wang] C

School of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, China<&wdkj&>College of Science, Central South University of Forestry and Technology, Changsha 410004, China

语种：

英文

关键词：

Carbon dioxide;Composite structures;Electronic structure;Fourier transform infrared spectroscopy;Free radicals;Metal-Organic Frameworks;Organometallics;Photocatalytic activity;Photoelectrons;Photons;Rhodium compounds;Spectrometers;X ray photoelectron spectroscopy;Catalytic performance;Fourier transform infrared spectrometer;Hydrothermal methods;Phosphomolybdic acid;Photo catalytic degradation;Photocatalytic reduction;Structure and morphology;UV-Vis diffuse reflectance spectroscopy;Rhodium metallography;carbon dioxide;carbon monoxide;free radical;metal organic framework;molybdic acid;rhodium;superoxide;Article;chemical structure;controlled study;cycling;degradation;diffuse reflectance spectroscopy;Fourier transform infrared spectroscopy;molecular stability;morphology;photocatalysis;priority journal;reduction (chemistry);synergistic effect;ultraviolet visible spectroscopy;X ray photoemission spectroscopy

期刊：

NEW JOURNAL OF CHEMISTRY

ISSN：

1144-0546

年：

2021

卷：

期：

页码：

7344-7352

DOI：

10.1039/d0nj06053d

基金类别：

This work was supported in part by the National Key R&D Program of China (2018YFB1501401).

机构署名：

本校为第一机构

院系归属：

材料科学与工程学院

理学院

摘要：

In this work, PMA@NH2-MIL-68(Rh) with a mangosteen spherical structure was successfully synthesized by a hydrothermal method for the photocatalytic reduction of carbon dioxide. The electronic structure and morphology of PMA@NH2-MIL-68(Rh) composites were characterized using Fourier transform infrared spectrometer (FTIR), X-ray photoelectron spectroscopy (XPS), and UV-Vis diffuse reflectance spectroscopy (UV-Vis DRS). Results showed that the 0.63% PMA@NH2-MIL-68(Rh) composite achieved the optimal catalytic performance, yielding 387.28 μmol·g−...

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The synergistic effect of phosphomolybdic acid on rhodium-based metal-organic frameworks for the efficient selective photocatalytic reduction of CO2to CO

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