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Automatic Pretreatment of Dispersive Liquid Liquid Microextraction Based on Immunomagnetic Beads Coupled with UPLC-FLD for the Determination of Zearalenone in Corn Oils

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成果类型:
期刊论文
作者:
Ni, Baoxia;Ye, Jin;Xuan, Zhihong;Li, Li;Wen, Xiangrui;...
通讯作者:
Liu, HM
作者机构:
[Ye, Jin; Li, Li; Wang, Songxue; Liu, HM; Xuan, Zhihong; Ni, Baoxia; Liu, Hongmei; Wen, Xiangrui; Li, Zongwang] Acad Natl Food & Strateg Reserv Adm, 11 Baiwanzhuang St, Beijing 100037, Peoples R China.
[Wen, Xiangrui] Cent South Univ Forestry & Technol, Coll Food Sci & Engn, Changsha 410004, Peoples R China.
[Li, Zongwang] Univ Shanghai Sci & Technol, Sch Hlth Sci & Engn, Shanghai 200093, Peoples R China.
通讯机构:
[Liu, HM ] A
Acad Natl Food & Strateg Reserv Adm, 11 Baiwanzhuang St, Beijing 100037, Peoples R China.
语种:
英文
关键词:
immunomagnetic beads;dispersive liquid liquid microextraction;pretreatment;zearalenone;corn oils;UPLC-FLD
期刊:
TOXINS
ISSN:
2072-6651
年:
2023
卷:
15
期:
5
页码:
337-
基金类别:
This research was funded by the Fundamental Research Funds for the Academy of National Food and Strategic Reserves Administration (ZX2205 and ZX2228), and the Young Elite Scientists Sponsorship Program by CAST (2021QNRC001).
机构署名:
本校为其他机构
院系归属:
食品科学与工程学院
摘要:
Sample pretreatment is a vital step in the detection of mycotoxins, and traditional pretreatment methods are time-consuming, labor-intensive and generate much organic waste liquid. In this work, an automatic, high-throughput and environmentally friendly pretreatment method is proposed. Immunomagnetic beads technology and dispersive liquid-liquid microextraction technology are combined, and the zearalenone in corn oils is directly purified and concentrated under the solubilization effects of surfactant. The proposed pretreatment method allows for the batch pretreatment of samples without pre-ex...

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