Two purified components from leaves of Camellia oleifera Abel, was extracted. With the spectrum of 1H-NMR, 13C-NMR, H-H COSY, DEPT-90, DEPT-135, HSQC and HMBC, they were analysized and identified. The two compounds are Dihydro-resveratrol (compound 1) and l-(3′, 5′-dimethoxy) phenyl-2-[4″-0-β-Z)-glucopyranosyl (6→1)-O-α-L-rhamnopyranosyl] phenylethane (compound 2). With 1H and 13C specturm, the number and affiliation of carbon and the hydrogen were elaborated. Compound 1 was first time achieved from family of Theaceae. Compound 2 was achi...