In this study, Box-Behnken design (BBD) was employed to optimize the process for H3PO4-activated Typha angustifolia activated carbon (TAC) production and Cr removal by TAC;the removal mechanisms were discussed based on TAC characterization, and the regeneration evaluation was also conducted. The optimum preparation conditions were activated time of 1.5 h, temperature of 469.02 °C, and incubation ratio of 4, resulting in an experimental carbon yield of 38.23% and Cr removal of 90.01%. The optimum adsorption parameters were found to be 0.02 g/50 mL TAC, 80 mg/L Cr(VI), and 2.21 pH with the o...