Taking Li3Sc(BO3)2 as host, a series of Eu3+/Tb3+ singly-doped and co-doped phosphors were synthesized through conventional solid-state reaction method. The phase assemblage and purity of as-prepared phosphors were investigated by analyzing their powder X-ray diffraction (XRD) patterns. The VUV-UV excited luminescence properties of a series of Eu3+/Tb3+ doped Li3Sc(BO3)2 phosphors were investigated in detail, with decay lifetime, chromaticity coordinate and mechanism of the phosphors analyzed. The luminescence decay lifetimes of Eu and Tb are b...