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Effect of preparation method on the surface properties and activity of Ni0.7Cu0.3Fe2O4 nanoparticles

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成果类型:
期刊论文
作者:
Tan, Xiaoyan;Li, Guiying;Zhao, Ying;Hu, Changwei*
通讯作者:
Hu, Changwei
作者机构:
[Hu, Changwei; Tan, Xiaoyan; Li, Guiying] Sichuan Univ, Key Lab Green Chem & Technol, Minist Educ, Coll Chem, Chengdu 610064, Sichuan, Peoples R China.
[Tan, Xiaoyan; Zhao, Ying] Cent S Univ Forestry & Technol, Inst Appl Chem, Changsha 412006, Hunan, Peoples R China.
通讯机构:
[Hu, Changwei] S
Sichuan Univ, Key Lab Green Chem & Technol, Minist Educ, Coll Chem, Chengdu 610064, Sichuan, Peoples R China.
语种:
英文
关键词:
BET surface area measurement;Coprecipitation method;Crystallization temperature;Cubic spinel structure;Decomposition process;Differential thermals;Direct oxidation;Experimental studies;Fourier transform infrared;Inductively coupled plasma spectroscopy;Milling methods;Octahedral sites;Preparation method;SEM;Single phase;Sol-gel combustion;Spinel formation;TEM;Temperature-programmed reduction;Thermal analysis;XPS;XRD analysis;Benzene;Benzene refining;Catalysis;Combustion;Diffraction;Gels;Hydrogen peroxide;Inductively coupled plasma;Infrared spectroscopy;Milling (machining);Nanoparticles;Nanostructured materials;Oxidation;Phenols;Precipitation (chemical);Scanning electron microscopy;Sol-gel process;Sol-gels;Sols;Surface properties;Thermoanalysis;Transmission electron microscopy;X ray diffraction;X ray diffraction analysis;X ray photoelectron spectroscopy
期刊:
Journal of Alloys and Compounds
ISSN:
0925-8388
年:
2010
卷:
493
期:
1-2
页码:
55-63
基金类别:
The financial support from the National Natural Science Foundation of China (No. 20072024 and No. 20502017 ), PCRIRT (No. IRT0846 ), determination for properties of catalysts from Analytical and Testing Center of Sichuan University are greatly appreciated.
机构署名:
本校为其他机构
院系归属:
理学院
摘要:
Ni0.7Cu0.3Fe2O4 nanoparticles were synthesized via sol-gel combustion technique, co-precipitation method and solid state milling method. Simultaneous thermogravimetric and differential thermal analysis (TG-DTA) was carried out to monitor the decomposition process of the precursors. The samples were characterized by Fourier transform infrared (FT-IR), inductively coupled plasma spectroscopy (ICPS), X-ray diffraction (XRD), BET surface area measurement, scanning electron microscopy (SEM), transmission electron microscopy (TEM), temperature progra...

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