In this research, compound biosorbent peanut shell‐HA (PSH) and millet chaff‐HA (MCH), which were composited by peanut shell (PS) and millet chaff (MC) with lead resistent Aspergillus oryzae (HA), respectively, were used to remove Pb2+ from aqueous solution. The characterize of biosorbents were analyzed by FTIR and SEM. Batch experiments were performed to evaluate the effect of pH, biosorbent concentration, initial Pb2+ concentration and contact time on the Pb2+ removal. The results indicated that the functional groups and surface morphology ...