Camellia oleifera meal is the byproduct of producing Camellia oil from seeds, and contains many bioactive components. In order to provide a theoretical basis for high efficient utilization of C. oleifera meal resources, after frozen, dried and water removal, C. oleifera meal was firstly extracted in ethanol by Soxhlet extraction method, and the extractives and extraction residues were vacuum concentrated and dried, and then were pyrolyzed at 600 ℃, and finally the compounds of the pyrolysates were analyzed by Py-GC/MS. The results showed that ...