In order to separate top value-added bioactive components from waste leaves of Phoenix tree and hence decrease its pollution to water environment, we attempted to analyze the chemical components of benzene/ethanol extractive of Phoenix leaves by means of GC/MS. Relative content of each component was determined by area normalization, and 10 compounds representing 94.37 % of the extractives were identified. The most abundant constituents were as: Ethanol, 2-butoxy-(47.49% from two peaks), exanoic acid, ethyl ester (22.89%), 1-Butyne, 3-chloro-(17.04%), Bicyclo[3.1.1]heptane, 2, 6, 6-trimethyl-(3...