A novel fluorescent lignin-based hydrogel with cellulose nanofibers and carbon dots (CDs) was synthesized for the high-value utilization of lignin and control of hexavalent chromium(Cr(VI)). Its chemical and physical structure was characterized, and its Cr(VI) sorption performance was evaluated. The results demonstrated that 3D porous structures were constructed in this hydrogel. The maximum adsorption capacity of this hydrogel was 599.9 mg/g, and its sorption performance met Freundlich and pseudo-second-order models. Meanwhile, this novel hydrogel exhibited high sensitivity to Cr(VI), with a ...